[1]戴晓雁,王玉洁,魏学兵.升血颗粒质量标准研究[J].西部中医药,2014,27(01):31-34.
 DAI Xiaoyan,WANG Yujie,WEI Xuebing.Study on Quality Standard of ShengXue Granules[J].Western Journal of Traditional Chinese Medicine,2014,27(01):31-34.
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升血颗粒质量标准研究
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
27
期数:
2014年01期
页码:
31-34
栏目:
方药·质量分析
出版日期:
2014-01-14

文章信息/Info

Title:
Study on Quality Standard of ShengXue Granules
文章编号:
1004-6852(2014)01-0031-04
作者:
戴晓雁1王玉洁1魏学兵2
1 甘肃省肿瘤医院,甘肃 兰州 730050; 2 甘肃省药品检验所
Author(s):
DAI Xiaoyan1 WANG Yujie1 WEI Xuebing2
1 Gansu Provincial Cancer Hospital, Lanzhou 730050, China; 2 Gansu Provincial Institute for Drug Control
关键词:
升血颗粒质量标准薄层色谱法高效液相色谱法
Keywords:
ShengXue granules quality control TLC HPLC
分类号:
R282.5
文献标志码:
A
摘要:
目的:建立升血颗粒的质量标准。方法:采用薄层色谱(TLC)法对升血颗粒中山茱萸、黄芪、丹参、麦门冬进行定性鉴别;采用高效液相色谱法对升血颗粒中马钱苷的含量进行定量测定。结果:TLC 斑点清晰、分离度好,阴性对照无干扰;马钱苷进样量在0.0752~0.451 μg/mL范围内与峰面积呈良好线性关系(r=0.998 3),平均加样回收率为96.2%,RSD=2.3%(n=6)。结论:所建立的标准可用于升血颗粒的质量控制。
Abstract:
Objective: To establish quality control of ShengXue granules. Methods: ShanZhuYu(Cornus officinalis), HuangQi(radix Astragalus), DanShen(radix salviae miltiorrhizae) and MaiMenDong [Ophitopogin japonicum (L.f) Ker.-Gawl.] in ShengXue granules were identified by TLC; the contents of loganin were determined by HPLC. Results: TCL figures were distinct and reproducible, the blank test showed no interference; loganin showed better linear relationship in the range between 0.0752 and 0.451 μg/mL and peak areas (r=0.998 3), average recovery rate was 96.2%, RSD=2.3% (n=6). Conclusion: The standard could be used in quality control of ShengXue granules.

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备注/Memo

备注/Memo:
收稿日期:2013-06-27作者简介:戴晓雁(1978—),女,主管中药师。研究方向:中药制剂。
更新日期/Last Update: 2014-01-15