[1]莫秋华,易东阳,耿耘,等.正交实验法优选茅苍术挥发油的提取工艺[J].西部中医药,2020,33(02):34-36.[doi:10.12174/j.issn.1004-6852.2020.02.09]
 MO Qiuhua,YI Dongyang,GENG Yun,et al.Extraction Process of Volatile Oil from Maocangzhu Optimized by Orthogonal Design[J].Western Journal of Traditional Chinese Medicine,2020,33(02):34-36.[doi:10.12174/j.issn.1004-6852.2020.02.09]
点击复制

正交实验法优选茅苍术挥发油的提取工艺
分享到:

《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
33
期数:
2020年02期
页码:
34-36
栏目:
出版日期:
2020-02-15

文章信息/Info

Title:
Extraction Process of Volatile Oil from Maocangzhu Optimized by Orthogonal Design
文章编号:
1004-6852(2020)02-0034-03
作者:
莫秋华易东阳耿耘刘睿颖马超英王兴
1 西南交通大学生命科学与工程学院,四川 成都610031; 2 重庆三峡医药高等专科学校; 3 重庆市抗肿瘤天然药物工程技术研究中心
Author(s):
MO Qiuhua 1, YI Dongyang 23△, GENG Yun 1, LIU Ruiying 1, MA Chaoying 1, WANG Xing 1
1School of Life Science and Engineering of Southwest Jiaotong University, Chengdu 610031, China;2Chongqing Three Gorges Medical College;3Chongqing Engineering Research Center of Antitumor Natural Drugs
关键词:
茅苍术挥发油提取工艺正交实验
Keywords:
Maocangzhu volatile oil extraction process orthogonal design
分类号:
R285.5
DOI:
10.12174/j.issn.1004-6852.2020.02.09
文献标志码:
A
摘要:
目的:优选出茅苍术挥发油的最佳提取工艺。方法:采用单因素和正交实验法,优化水蒸气蒸馏法提取茅苍术挥发油的提取工艺,以挥发油的提取率为指标,考察料液比、浸泡时间、提取时间对挥发油提取率的影响。结果:茅苍术挥发油的最佳提取工艺料液比为1∶10,不浸泡,超声30 min,提取8 h,茅苍术挥发油收率为4.80%,3次提取的RSD值为1.25%。结论:该提取工艺稳定可行,准确合理,为茅苍术挥发油的提取工艺提供了理论依据。
Abstract:
Objective: To optimize the best extraction process of volatile oil from Maocangzhu (Atreactylo-dis Rhizoma). Methods: Single-factor and orthogonal design were used to optimize the extraction process of volatile oil from Maocangzhu by steam distillation, by taking the extraction rate of volatile oil as the index, the influence of material - to - liquid ratio, soaking time and extraction time were surveyed on the extraction yield of volatile oil. Results: The best material - to - liquid ratio of volatile oil from Maocangzhu was 1∶10, no soaking, ultrasound for 30minutes, extracting for eight hours, extraction yield of volatile oil was 4.80%, RSD value of three times extraction was 1.25%. Conclusion: The extraction process, stable, feasible, accurate and rational, could provide theoretical evidence for the extraction of volatile oil from Maocangzhu.

相似文献/References:

[1]李冬华,马潇,宋平顺,等.三种方法提取当归挥发性成分的气相色谱-质谱联用分析[J].西部中医药,2013,26(08):15.
 LI Donghua,MA Xiao,SONG Pingshun,et al.Analysis of Three Methods for Extracting Volatile Constituent from DangGui by Combination of Gas Chromatography and Mass Spectrometry[J].Western Journal of Traditional Chinese Medicine,2013,26(02):15.
[2]金国泰,李 博,王树荣△.柴胡解热的物质基础、药效及机制研究[J].西部中医药,2014,27(02):20.
 JIN Guotai,LI Bo,WANG Shurong.Research on the Mechanism, the Effects and Material Foundation of ChaiHu in Relieving Fever[J].Western Journal of Traditional Chinese Medicine,2014,27(02):20.
[3]焦凯,张建强,魏玉辉△,等.平胃散挥发油促进大鼠胃排空作用药效物质的筛选[J].西部中医药,2013,26(09):20.
 JIAO Kai,ZHANG Jianqiang,WEI Yuhui,et al.Screening of Active Substance from Volatile Oil of PingWeiSan on Gastric Emptying of Rats[J].Western Journal of Traditional Chinese Medicine,2013,26(02):20.
[4]李明珠,宋平顺△,赵建邦.藏药烈香杜鹃花和叶中挥发性成分的GC-MS分析[J].西部中医药,2016,29(01):36.
 LI Mingzhu,SONG Pingshun,ZHAO Jianbang.Analysis of Volatile Components in Tibetan Medicine LieXiang DuJuan by GC-MS[J].Western Journal of Traditional Chinese Medicine,2016,29(02):36.
[5]高小恒,李莎莎,陈达艳,等.玉红膏挥发油化学成分GC-MS分析[J].西部中医药,2020,33(01):60.[doi:10.12174/j.issn.1004-6852.2020.01.16]
 GAO Xiaoheng,LI Shasha,CHEN Dayan,et al.Chemical Ingredients Analysis of Volatile Oil from Yuhong Plaster by GC-MS[J].Western Journal of Traditional Chinese Medicine,2020,33(02):60.[doi:10.12174/j.issn.1004-6852.2020.01.16]
[6]李凤,练志辉,张浩怡,等.厚朴不同炮制品中挥发性成分比较[J].西部中医药,2020,33(07):33.[doi:10.12174/j.issn.1004-6852.2020.07.08]
 LI Feng,LIAN Zhihui,ZHANG Haoyi,et al.Comparisons of Volatile Ingredients Contained in Different Processed Products of Houpo[J].Western Journal of Traditional Chinese Medicine,2020,33(02):33.[doi:10.12174/j.issn.1004-6852.2020.07.08]

备注/Memo

备注/Memo:
收稿日期:2019-04-19*基金项目:重庆市基础与前沿研究计划项目(cstc2014jcyjA10116)。作者简介:莫秋华(1994—),女,在读硕士研究生。研究方向:中药物质基础及作用机理。通讯作者:易东阳(1973—),男,硕士学位,教授。研究方向:中药物质基础及作用机理。
更新日期/Last Update: 2020-02-15