[1]毛和平,刘光斌,石晓峰,等.柴胡舒肝健乳丸质量标准研究[J].西部中医药,2013,26(10):31-33.
　MAO Heping,LIU Guangbin,SHI Xiaofeng,et al.Study on Quality Standard of ChaiHu ShuGan JianRuWan[J].Western Journal of Traditional Chinese Medicine,2013,26(10):31-33.
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柴胡舒肝健乳丸质量标准研究
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
26
期数:
2013年10期
页码:
31-33
栏目:
出版日期:
2013-10-15

文章信息/Info

Title:
Study on Quality Standard of ChaiHu ShuGan JianRuWan
文章编号:
1004-6852(2013)10-0031-03
作者:
毛和平1，刘光斌1，石晓峰2，冯丽红1，韩晓莉1
1 酒钢医院，甘肃 嘉峪关 735100； 2 甘肃省医学科学研究院
Author(s):
MAO Heping1, LIU Guangbin1, SHI Xiaofeng2, FENG Lihong1, HAN Xiaoli1
1 JiuGang Hospital, Jiayuguan 735100, China; 2 Gansu Provincial Academy of Medical Science
关键词:
柴胡舒肝健乳丸; HPLC; 芍药苷
Keywords:
ChaiHu ShuGan JianRuWan;  HPLC;  peoniflorin
分类号:
R282
文献标志码:
A
摘要:
目的：建立柴胡舒肝健乳丸的质量标准。方法：采用薄层色谱法(TCL)法对柴胡舒肝健乳丸中柴胡、丹参、香附、夏枯草进行定性鉴别，采用高效液相色谱法(HPLC)法对柴胡舒肝健乳丸中芍药苷进行定量分析。结果：薄层色谱斑点清晰，专属性强；芍药苷对照品在0.0057～0.0570 mg/mL浓度范围内与峰面积呈良好的线性关系(r=0.999 9)，平均加样回收率为100.25%，RSD=1.66%(n=9)。结论：本质量标准方法简单、操作简便、结果准确、重复性好，可用于柴胡舒肝健乳丸的质量控制。
Abstract:
Objective: To establish quality standard for ChaiHu ShuGan JianRuWan. Method: ChaiHu (Radix Bupleur), DanShen(Radix Salviae Miltiorrhizae), XiangFu(rhizoma cyperi), XiaKuCao(Prunellae Spica) in ChaiHu ShuGan JianRuWanwere identified by TLC, peoniflorin of ChaiHu ShuGan JianRuWan was analyzed quantitatively. Result: TCL figures were clear with strong pecialization; peoniflorin showed better linear relationship in the range between 0.0057 and 0.0570 mg/mL and peak area(r=0.999 9), average recovery rate was 100.25%, RSD=1.66% (n=9). Conclusion: The method for quality standard is simple, feasible, accurate and reproducible, which could be used for quality control of ChaiHu ShuGan JianRuWan.

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备注/Memo

备注/Memo:
收稿日期：2013-02-15 作者简介：毛和平(1965—)，男，副主任中药师。研究方向：中药制剂。
更新日期/Last Update: 2013-10-15