[1]吴忠民,贾 忠△,李喜香,等.黄芪党参颗粒中黄芪甲苷含量的HPLC测定方法[J].西部中医药,2012,25(10):23-25.
 WU Zhong-min,JIA Zhong,LI Xi-xiang,et al.HPLC Determination of Astragaloside Ⅳ in HuangQi DangShen Granule[J].Western Journal of Traditional Chinese Medicine,2012,25(10):23-25.
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黄芪党参颗粒中黄芪甲苷含量的HPLC测定方法()
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
25
期数:
2012年10期
页码:
23-25
栏目:
出版日期:
2012-10-15

文章信息/Info

Title:
HPLC Determination of Astragaloside Ⅳ in HuangQi DangShen Granule
文章编号:
1004-6852(2012)10-0023-03
作者:
吴忠民1贾  忠2△李喜香3高满义4
1 武威市第二人民医院,甘肃 武威 733009; 2 兰州市肺科医院药剂科; 3 甘肃省中医院药剂科; 4 甘肃陇西正大药业有限公司
Author(s):
WU Zhong-min1, JIA Zhong2△, LI Xi-xiang3, GAO Man-yi4
1  The People′s Second Hospital of Wuwei, Wuwei 733009, China;  2  Pharmacy of Lanzhou Pulmonary Hospital; 3  Pharmacy of Gansu Province Hospital of Traditional Chinese Medicine;
4  Gansu Longxi Zhengda Pharmaceutical Co. Ltd
关键词:
[关键词] 黄芪党参颗粒黄芪甲苷含量测定HPLC
Keywords:
Keywords  HuangQi DangShen granule Astragaloside Ⅳ determination HPLC
分类号:
R285
文献标志码:
A
摘要:
[摘  要] 目的:建立黄芪党参颗粒中黄芪甲苷含量的HPLC测定方法。方法:以ELSD为检测器,色谱柱C18(Alltech Hypersil ODS 4.6 mm×150 mm,5 μm);流动相:乙腈∶水(40∶60),流速:1.0 mL/min;柱温:25℃;漂移管温度:100℃,载气量:2.6 L/min。结果:回归方程y= 1.5471x+ 2.6231(r=0.9996),黄芪甲苷在1.656~4.968μg/ mL之间峰面积与浓度线性关系良好。平均回收率为101%。结论:该法简便可靠,可为黄芪党参颗粒质量控制提供依据。
Abstract:
Abstract  Objective: To establish a method for content determination of astragaloside Ⅳ in HuangQi DangShen granule with HPLC. Method: ELSD was taken as detector, chromatographic column was C18 (Alltech Hypersil ODS 4.6 mm×150 mm, 5 μm); mobile phase: methyl cyanide-water(40∶60), flow rate: 1.0 mL/min; column temperature: 25℃; drift tube temperature: 100℃, containing gas 2.6 L/min. Result: The regression equation was y= 1.5471x+ 2.6231(r=0.9996). The excellent linear ranges was 1.656~4.968 μg/mL. Average recovery rate was 101%. Conclusion: The method, simple and reliable, could provide evidence for quality control of HuangQi DangShen granule.

参考文献/References:

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更新日期/Last Update: 2012-12-19