[1]魏文芝,海平,卢永昌.藏成药萨热十三味鹏鸟丸的质量控制[J].西部中医药,2020,33(02):26-28.[doi:10.12174/j.issn.1004-6852.2020.02.07]
　WEI Wenzhi,HAI Ping,LU Yongchang.Quality Control for Tibetan Medicine Sare Shisanwei Pengniao Pills[J].Western Journal of Traditional Chinese Medicine,2020,33(02):26-28.[doi:10.12174/j.issn.1004-6852.2020.02.07]
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藏成药萨热十三味鹏鸟丸的质量控制
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
33
期数:
2020年02期
页码:
26-28
栏目:
出版日期:
2020-02-15

文章信息/Info

Title:
Quality Control for Tibetan Medicine Sare Shisanwei Pengniao Pills
文章编号:
1004-6852(2020)02-0026-03
作者:
魏文芝，海平，卢永昌
1 青海省药品检验检测院/青海省中藏药现代化研究重点实验室，青海 西宁 810016；2 青海民族大学药学院
Author(s):
WEI Wenzhi 1, HAI Ping 1, LU Yongchang 2
1Qinghai Provincial Drug Inspection and Testing Institute/Qinghai Provincial Key Laboratory of Traditional Chinese and Tibetan Medicine Modernization Research, Xining 810016, China; 2College of Pharmacy, Qinghai University for Nationalities
关键词:
萨热十三味鹏鸟丸; 显微鉴别; 化学鉴别; 高效液色相谱法; 含量测定; 去氢二异丁香酚; 丁香; 磁石; 藏药
Keywords:
Sare Shisanwei Pengniao pills;  microscopic identification;  chemical identification;  HPLC; content determination;  dehydrodiisobuterol;  Dingxiang;  Cishi;  Tibetan medicine
分类号:
R285
DOI:
10.12174/j.issn.1004-6852.2020.02.07
文献标志码:
A
摘要:
目的：建立藏成药萨热十三味鹏鸟丸的质量控制方法。方法：采用显微鉴别法对丁香进行鉴别，采用化学鉴别法对磁石进行鉴别；采用高效液相色谱法测定成药中去氢二异丁香酚含量。结果：丁香、磁石的鉴别方法斑点清晰，反应灵敏，阴性无干扰，具有较好的专属性；去氢二异丁香酚在0.041 83～209.1 mg/L范围内线性关系良好(r=0.999 6)，平均回收率为101.27%，RSD为1.35%；结论：所建立的方法定性定量准确，重现性好，可有效控制该藏成药的制剂质量。
Abstract:
Objective: To establish the method for quality control of Tibetan medicine Sare Shisanwei Pengniao pills. Methods: Microscopic identification was used to distinguish Dingxiang (caryophylli flos), chemical identification to distinguish Cishi (magnetitum), HPLC to measure the contents of dehydrodiisobuterol contained in Tibetan medicine. Results: The identification methods of Dingxiang and Cishi were distinct, sensitive, negative and specific, and the blank test showed no interference; dehydrodiisobuterol presented good linear relationship in the range from 0.041 83 to 209.1 mg/L, average recovery rate was 101.27%, RSD was 1.35%. Conclusion: The method, qualitative, quantitative, accurate and reproducible, could effectively control the quality of Tibetan medicine

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备注/Memo

备注/Memo:
收稿日期：2019-04-06*基金项目：青海省药品检验检测平台项目；青海省科技厅科研基础条件平台项目(2017-ZJ-Y40)；青海省科学技术成果(9632015Y0281)。作者简介：魏文芝(1984—)，女，硕士学位，副主任药师。研究方向：药物分析、药品标准提高。
更新日期/Last Update: 2020-02-15