[1]陈永新,李静文,李峰△.木瓜中脂肪酸成分和其他脂溶性成分的气-质联用分析[J].西部中医药,2016,29(05):31-33.
CHEN Yongxin,LI Jingwen,LI Feng.Analysis of Fatty Acid and Other Liposoluble Components in Pawpaw by GC-MS[J].Western Journal of Traditional Chinese Medicine,2016,29(05):31-33.
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木瓜中脂肪酸成分和其他脂溶性成分的气-质联用分析(
)
《西部中医药》[ISSN:2096-9600/CN:62-1204/R]
- 卷:
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29
- 期数:
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2016年05期
- 页码:
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31-33
- 栏目:
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- 出版日期:
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2016-05-15
文章信息/Info
- Title:
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Analysis of Fatty Acid and Other Liposoluble Components in Pawpaw by GC-MS
- 文章编号:
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1004-6852(2016)05-0031-03
- 作者:
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陈永新1，李静文2，李峰3△
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1 新乡医学院第二附属医院，河南 新乡 453002；2 临淄区食品药品监督管理局； 3 山东中医药大学药学院
- Author(s):
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CHEN Yongxin1, LI Jingwen2, LI Feng3△
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1 The Second Affiliated Hospital of Xinxiang Medical University, Xinxiang 453002, China;
2 Linzi District of Food and Drug Supervision Administration Bureau;
3 Pharmacy School of Shandong University of Traditional Chinese Medicine
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- 关键词:
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木瓜; 脂肪酸; 脂溶性成分; 气相色谱-质谱联用
- Keywords:
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pawpaw; fatty acid; liposoluble components; GC-MS
- 分类号:
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R285.5
- 文献标志码:
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A
- 摘要:
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目的：分析和鉴定木瓜中脂肪酸及其他脂溶性成分。方法：木瓜粉碎后过40目筛，用石油醚(60～90℃)回流提取，提取液经浓缩后进行甲酯化，采用GC-MS法对其脂肪酸及其他脂溶性成分进行分析和鉴定。结果：从木瓜石油醚提取物中检测出13种物质，鉴定出其中的4种脂肪酸和8种非脂肪酸成分。结论：木瓜中的主要脂肪酸成分为14-甲基-十五酸(15.21%)、油酸(34.79%)、亚油酸(14.72%)和硬脂酸甲酯(2.59%)。
- Abstract:
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Objective: To analyze and identify fatty acid and other liposoluble components in pawpaw (Fructus Chaenomelis). Methods: Pawpaw was smeared and screened by 40 meshes, refluxed and extracted by petroleum benzin (60~90℃), the extraction underwent esterification after condensed, fatty acid and other liposoluble components in pawpaw were analyzed and identified by GC-MS. Results: Altogether 13 kinds of organic compounds were found in the extract of pawpaw, four kinds of fatty acids and eight kinds of non fatty acids were identified. Conclusion: Main fatty acids in pawpaw are 14-methyl-Pentadecanoic acid (15.21%), 9-(Z)-Octadecenoie acid (34.79%), 9, 12-(Z, Z)-Octadecadienoie acid (14.72%) and Octadecanoic acid (2.59%).
备注/Memo
- 备注/Memo:
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收稿日期：2015-02-03*基金项目：国家重点基础研究发展计划(“973”计划)项目(编号2007CB512601)。作者简介：陈永新(1982—)，男，硕士学位，中药师。研究方向：临床药学。△通讯作者：李峰(1957—)，男，博士研究生导师，博士学位，教授。研究方向：中药质量控制。
更新日期/Last Update:
2016-05-15