[1]李冬华,张平,张明童,等.两种初加工方法当归饮片中不同提取成分的指纹图谱分析[J].西部中医药,2021,34(02):39-45.[doi:10.12174/j.issn.2096-9600.2021.02.10]
　LI Donghua,ZHANG Ping,ZHANG Mingtong,et al.Comparison of Fingerprints of Different Components Extracted from Danggui Pieces Processed by Different Methods[J].Western Journal of Traditional Chinese Medicine,2021,34(02):39-45.[doi:10.12174/j.issn.2096-9600.2021.02.10]
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两种初加工方法当归饮片中不同提取成分的指纹图谱分析
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
34
期数:
2021年02期
页码:
39-45
栏目:
出版日期:
2021-02-15

文章信息/Info

Title:
Comparison of Fingerprints of Different Components Extracted from Danggui Pieces Processed by Different Methods
作者:
李冬华1,2, 张平1,2, 张明童1,2, 杨静1,2, 马潇1,2, 宋平顺1,2, 杨平荣1,2
1.甘肃省药品检验研究院，甘肃 兰州 730070
2.国家药品监督管理局中药材及饮片质量控制重点实验室
Author(s):
LI Donghua1,2, ZHANG Ping1,2, ZHANG Mingtong1,2, YANG Jing1,2, MA Xiao1,2, SONG Pingshun1,2, YANG Pingrong1,2
1.Gansu Institute for Drug Control, Lanzhou 730070, China
2.State Drug Administration Key Laboratory of Quality Control of Chinese Medicinal Materials and Decoction Pieces
关键词:
当归饮片; 初加工; 液相色谱; 气相色谱; 指纹图谱; 相似度
Keywords:
pieces; primary processing; HPLC; gas chromatography; fingerprint; similarity
分类号:
R283
DOI:
10.12174/j.issn.2096-9600.2021.02.10
摘要:
目的比较两种初加工方法，传统烟熏干燥法和现代控温控湿干燥法所生产的当归饮片中不同提取成分的指纹图谱。 方法提取当归饮片中挥发油成分、醇溶性成分和水溶性成分，分别以阿魏酸对照品和藁本内酯对照品作为参照物，利用国家药典委员会颁布的“中药色谱指纹图谱相似度评价系统”软件进行分析。 结果两种初加工方法的当归饮片中3种提取成分的相似度分别为0.998、0.987、0.936，表明两种初加工方法所生产的当归饮片整体化学特征较为近似，所含成分没有明显差别，不会影响其质量和功效。 结论考虑到环境保护和现代规模化生产模式，应该提倡现代控温控湿干燥法作为新型初加工方法，并加以推广。
Abstract:
ObjectiveTo compare the fingerprints of different components extracted from Danggui pieces processed by traditional smoke drying method and modern temperature and humidity control drying method. MethodsAfter extracting volatile constituents, alcohol soluble components and water soluble components from Danggui pieces, ferulic acid reference substance and ligustilide reference substance were taken as the objects of reference, similarity evaluation system of chromatographic fingerprint of traditional Chinese Medicine issued by Chinese pharmacopoeia commission was used to perform the analysis. ResultsThe similarity degrees of three extracting components from Danggui pieces processed by two methods were 0.998, 0.987 and 0.936 respectively, which demonstrated that chemical characteristics of Danggui pieces produced by the two methods were similar, no significant difference was found in the compositions, and it will not affect its quality and efficacy. ConclusionIn consideration of environmental protection and modern large-scale production mode, modern temperature and humidity control drying method should be recommended as new primary processing method and extended.

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备注/Memo

备注/Memo:
李冬华（1977—），女，硕士研究生，副主任药师。研究方向：中药检验、标准研究及资源利用。甘肃省食品药品重点研发项目（2017GSFDA012，2017GSFDA017）；甘肃省教育厅科技创新团队建设项目（2016C-05）。
更新日期/Last Update: 2021-02-15