[1]成 瑞,鞠爱华△,白万富,等.蒙药牛胆粉反相高效液相色谱指纹图谱研究*[J].西部中医药,2014,27(02):25-28.
　CHENG Rui,JU Aihua,BAI Wanfu,et al.Study on Fingerprint of Mongolian Medicine NiuDanFen by RP-HPLC[J].Western Journal of Traditional Chinese Medicine,2014,27(02):25-28.
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蒙药牛胆粉反相高效液相色谱指纹图谱研究*
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
27
期数:
2014年02期
页码:
25-28
栏目:
出版日期:
2014-02-15

文章信息/Info

Title:
Study on Fingerprint of Mongolian Medicine NiuDanFen by RP-HPLC
文章编号:
1004-6852(2014)02-0025-04
作者:
成 瑞1，鞠爱华2△，白万富2，张慧文2，周秀娟2
1 内蒙古医科大学第一附属医院，内蒙古 呼和浩特 010050； 2 内蒙古医科大学药学院
Author(s):
CHENG Rui1, JU Aihua2△, BAI Wanfu2, ZHANG Huiwen2, ZHOU Xiujuan2
1 The First Affiliated Hospital to Inner Mongolia Medical University, Hohhot 010050, China; 2 The College of Pharmacy of Inner Mongolia Medical University
关键词:
牛胆粉; 指纹图谱; 反相高效液相色谱法
Keywords:
NiuDanFen;  fingerprint;  RP-HPLC
分类号:
R282.5
文献标志码:
A
摘要:
采用梯度洗脱的反相高效液相色谱法(RPLC)，首次建立了10批不同产地、不同批次牛胆粉药材由17种成分组成的色谱指纹图谱。本研究所建立的牛胆粉RPLC指纹图谱从试样提取的精密度、稳定性、图谱重复性等方面均符合《中药注射剂指纹图谱研究的技术要求(暂行)》中的有关规定，该方法具有重现性好，特征性强，方法简便、快速等特点，可用于牛胆粉药材真伪鉴别和质量评价。
Abstract:
chromatographic fingerprints of ten batches of NiuDanFen(Pulvis Billis Bovis) from different producing areas and different batches including 17 kinds of ingredients were initially established by adopting reversed-phase high performance liquid chromatography(RP-HPLC)with gradient elution. The accuracy, stability and fingerprint repeatability of fingerprint conformed to the regulations in Technical requirements of herbal injection fingerprint study, the method, reproducible, convenient and rapid, others, could be used in the differentiation and quality assessment of NiuDanFen.

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备注/Memo

备注/Memo:
收稿日期：2013-05-10*基金项目：内蒙古自治区蒙药现代化重大科技专项资助项目(编号MX2005ZB001)作者简介：成瑞(1964—)，女，副主任医师。研究方向：医院药学研究。△通讯作者：鞠爱华(1955—)，女，硕士研究生导师，教授。研究方向：中蒙药鉴别、质量标准及新药研发。
更新日期/Last Update: 2014-02-15