[1]戴晓雁,王玉洁,魏学兵.升血颗粒质量标准研究[J].西部中医药,2014,27(01):31-34.
　DAI Xiaoyan,WANG Yujie,WEI Xuebing.Study on Quality Standard of ShengXue Granules[J].Western Journal of Traditional Chinese Medicine,2014,27(01):31-34.
点击复制

升血颗粒质量标准研究
分享到：

《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
27
期数:
2014年01期
页码:
31-34
栏目:
出版日期:
2014-01-14

文章信息/Info

Title:
Study on Quality Standard of ShengXue Granules
文章编号:
1004-6852(2014)01-0031-04
作者:
戴晓雁1，王玉洁1，魏学兵2
1 甘肃省肿瘤医院，甘肃 兰州 730050； 2 甘肃省药品检验所
Author(s):
DAI Xiaoyan1, WANG Yujie1, WEI Xuebing2
1 Gansu Provincial Cancer Hospital, Lanzhou 730050, China; 2 Gansu Provincial Institute for Drug Control
关键词:
升血颗粒; 质量标准; 薄层色谱法; 高效液相色谱法
Keywords:
ShengXue granules;  quality control;  TLC;  HPLC
分类号:
R282.5
文献标志码:
A
摘要:
目的：建立升血颗粒的质量标准。方法：采用薄层色谱(TLC)法对升血颗粒中山茱萸、黄芪、丹参、麦门冬进行定性鉴别；采用高效液相色谱法对升血颗粒中马钱苷的含量进行定量测定。结果：TLC 斑点清晰、分离度好，阴性对照无干扰；马钱苷进样量在0.0752～0.451 μg/mL范围内与峰面积呈良好线性关系(r＝0.998 3)，平均加样回收率为96.2％，RSD＝2.3％(n＝6)。结论：所建立的标准可用于升血颗粒的质量控制。
Abstract:
Objective: To establish quality control of ShengXue granules. Methods: ShanZhuYu(Cornus officinalis), HuangQi(radix Astragalus), DanShen(radix salviae miltiorrhizae) and MaiMenDong [Ophitopogin japonicum (L.f) Ker.-Gawl.] in ShengXue granules were identified by TLC; the contents of loganin were determined by HPLC. Results: TCL figures were distinct and reproducible, the blank test showed no interference; loganin showed better linear relationship in the range between 0.0752 and 0.451 μg/mL and peak areas (r=0.998 3), average recovery rate was 96.2%, RSD=2.3% (n=6). Conclusion: The standard could be used in quality control of ShengXue granules.

相似文献/References:

[1]孙绪丁,任松鹏,刘玉芹.如意珍宝丸质量标准研究[J].西部中医药,2013,26(01):24.
　SUN Xuding,REN Songpeng,LIU Yuqin.Study on Quality Standard of RuY i ZhenBaoWan[J].Western Journal of Traditional Chinese Medicine,2013,26(01):24.
[2]闫旭,景明△,陈晖,等.儿童排铅咀嚼片的质量标准研究*[J].西部中医药,2012,25(11):28.
　YANXu,JING Ming,CHEN Hui,et al.Study on Quality Standard of Lead-removing Tablets for Children[J].Western Journal of Traditional Chinese Medicine,2012,25(01):28.
[3]张涛,景明△.归芪通便颗粒的质量标准研究*[J].西部中医药,2013,26(03):31.
　ZHANG Tao,JING Ming,Study on Quality Standard of GuiQi TongBian Granules[J].Western Journal of Traditional Chinese Medicine,2013,26(01):31.
[4]何静,高军,安晔.地补更年安颗粒质量标准研究[J].西部中医药,2014,27(09):24.
[5]毛和平,路宁维,谢六生,等.乳没接骨丸质量标准研究*[J].西部中医药,2015,28(01):18.
[6]王帆,孙岩,杨玉华.无糖型黄疸茵陈颗粒的质量标准研究[J].西部中医药,2015,28(06):32.[doi:2015/6/16 0:00:00]
[7]王建平,曾海松,俞洁东,等.虎力散胶囊的质量标准再研究[J].西部中医药,2015,28(07):20.
[8]李靖,路莎莎.高效液相色谱法测定愈伤胶囊中三七总皂苷和延胡索乙素的含量[J].西部中医药,2015,28(10):46.
[9]任一杰,张 华△,张喜民,等.复方金银花滴丸质量标准的研究[J].西部中医药,2014,27(06):16.
　REN Yijie,ZHANG Hua,ZHANG Ximin,et al.Study on Quality Standard for Compound JinYinHua Dripping Pills[J].Western Journal of Traditional Chinese Medicine,2014,27(01):16.
[10]杨志军,张文丽△,贾忠,等.虫创愈胶囊的质量标准研究[J].西部中医药,2014,27(11):28.
[11]戴晓雁,王玉洁,魏学兵.升血颗粒质量标准的研究[J].西部中医药,2013,26(09):31.
　DAI Xiaoyan,WANG Yujie,WEI Xuebing.Study on Quality Standard of ShengXue Granules[J].Western Journal of Traditional Chinese Medicine,2013,26(01):31.

备注/Memo

备注/Memo:
收稿日期：2013-06-27作者简介：戴晓雁(1978—)，女，主管中药师。研究方向：中药制剂。
更新日期/Last Update: 2014-01-15