[1]戴晓雁,王玉洁,魏学兵.升血颗粒质量标准的研究[J].西部中医药,2013,26(09):31-33.
 DAI Xiaoyan,WANG Yujie,WEI Xuebing.Study on Quality Standard of ShengXue Granules[J].Western Journal of Traditional Chinese Medicine,2013,26(09):31-33.
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升血颗粒质量标准的研究
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
26
期数:
2013年09期
页码:
31-33
栏目:
方药·质量分析
出版日期:
2013-09-15

文章信息/Info

Title:
Study on Quality Standard of ShengXue Granules
文章编号:
1004-6852(2013)09-0031-03
作者:
戴晓雁1王玉洁1魏学兵2
1 甘肃省肿瘤医院,甘肃 兰州 730050;2 甘肃省药检所
Author(s):
DAI Xiaoyan1 WANG Yujie1 WEI Xuebing2
1 Gansu Provincial Cancer Hospital, Lanzhou 730050, China; 2 Gansu Province Institute for Food and Drug Control
关键词:
升血颗粒质量标准薄层色谱法高效液相色谱法
Keywords:
ShengXue granules quality standard thin-layer chromatography (TLC) high performance liquid chromatography (HPLC)
分类号:
R284
文献标志码:
A
摘要:
目的:建立升血颗粒的质量标准。方法:采用薄层色谱(TLC)法对处方中山茱萸、黄芪、丹参、麦门冬进行定性鉴别;采用高效液相色谱法对制剂中马钱苷的含量进行定量测定。结果:TLC斑点清晰、分离度好,阴性对照无干扰;马钱苷进样量在0.075 2~0.451μg/mL范围内与峰面积呈良好线性关系(r=0.998 3),平均加样回收率为96.2%,RSD=2.3%(n=6)。结论:所建立的标准可用于升血颗粒的质量控制。
Abstract:
Objective: To establish quality standard for ShengXue granules. Method: The herbs including ShanZhuYu(Fructus Corni), HuangQi (radix astragali), DanShen(Salvia miltiorrhiza) and MaiMengDong (Radix Ophiopogonis) in the prescription were identified qualitatively through thin-layer chromatography (TLC); loganin contents were determined qualitatively by high performance liquid chromatography (HPLC). Result: TCL spotting was clear with high resolution and the blank test showed no interference; the sample size of loganin showed better linear relationship in the range of 0.0752 to 0.451 μg/mL and peak area (r=0.998 3), average recovery rate was 96.2%, RSD=2.3% (n=6). Conclusion: The established standard could be used for quality control of ShengXue granules.

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备注/Memo

备注/Memo:
收稿日期:2013-04-25
更新日期/Last Update: 2013-09-15