[1]鱼光强,高晔珩△.强力感冒片指纹图谱的初步研究[J].西部中医药,2015,28(01):23-25.
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强力感冒片指纹图谱的初步研究
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《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
28
期数:
2015年01期
页码:
23-25
栏目:
出版日期:
2015-01-15

文章信息/Info

文章编号:
1004-6852(2015)01-0023-03
作者:
鱼光强高晔珩△
榆林市食品药品检验所,陕西 榆林 719000
关键词:
强力感冒片绿原酸高效液相色谱法指纹图谱
分类号:
R284.11
摘要:
目的:研究强力感冒片的HLPC指纹图谱。方法:采用HLPC方法测定,色谱柱:KromasilODS-2 C18(250 mm×4.6 mm,5 μm);检测波长:327 nm;流速:1.0 mL/min;柱温:25℃;乙腈-0.4%的磷酸水溶液(12:88)为流动相。结果:确定了7个共有峰,5批样品每批处理两份,10份样品指纹图谱的相似度均在0.9以上,绿原酸的线性范围为0.03~0.33 μg/mL,加样回收率为 101.27%。结论:所建立的HLPC简便可靠,可用于强力感冒片的质量控制。

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备注/Memo

备注/Memo:
作者简介:鱼光强(1986—),男,硕士学位,药师。研究方向:中药提取。△通讯作者:高晔珩(1962—),女,主任药师。研究方向:中药鉴定。
更新日期/Last Update: 2015-01-15