[1]焦正花,刘燕珺,李文萍.正交实验优选黄连解毒合剂的工艺研究*[J].西部中医药,2014,27(10):26.
点击复制

正交实验优选黄连解毒合剂的工艺研究*
分享到:

《西部中医药》[ISSN:2096-9600/CN:62-1204/R]

卷:
27
期数:
2014年10期
页码:
26
栏目:
出版日期:
2014-10-15

文章信息/Info

作者:
焦正花1刘燕珺2李文萍1
1 甘肃省中医院药剂科,甘肃 兰州 730050; 2 嘉峪关市药品检验所
关键词:
黄连解毒合剂黄芩苷高效液相色谱法正交实验
摘要:
目的:优选黄连解毒合剂提取工艺的最佳条件。方法:以干膏、黄芩苷为评价指标,用正交实验法对黄连解毒合剂进行制备工艺的筛选。结果:最佳提取工艺为煎煮2次,每次加水8倍,第1次1小时,第2次0.5小时,醇沉浓度为55%。结论:该优选工艺合理可行。

相似文献/References:

[1]郭敏,姜华,肖正国.高效液相色谱法同时测定三黄中空栓中黄芩苷、盐酸小檗碱的含量*[J].西部中医药,2014,27(09):19.
[2]张立峰.RP-HPLC法同时测定清热止嚏颗粒中黄芩苷、芍药苷和葛根素[J].西部中医药,2015,28(04):27.
[3]王帆,孙岩,杨玉华.无糖型黄疸茵陈颗粒的质量标准研究[J].西部中医药,2015,28(06):32.[doi:2015/6/16 0:00:00]
[4]王林凤,魏国玲,康毅.蒲地兰颗粒的质量控制[J].西部中医药,2014,27(04):17.
 WANG Linfeng,WEI Guoling,KANG Yi.Quality Control of PuDiLan Granules[J].Western Journal of Traditional Chinese Medicine,2014,27(10):17.
[5]李彩东,王信,潘新波,等.波长切换技术同时测定加味小柴胡汤胶囊中党参炔苷等4种成分[J].西部中医药,2017,30(01):26.
 LI Caidong,WANG Xin,PAN Xinbo,et al.Detection of Four Kinds of Ingredients in Modified Xiao ChaiHu Capsules by HPLC Wavelength Switching Method Simultaneously[J].Western Journal of Traditional Chinese Medicine,2017,30(10):26.
[6]杨小军,丁永辉.RP-HPLC法测定牛黄上清丸中栀子苷、芍药苷、黄芩苷、小檗碱的含量[J].西部中医药,2016,29(02):27.
 YANG Xiaojun,DING Yonghui.Determination of Jasminoidin, Peoniflorin, Baicalin and Berberine Hydrochloride in NiuHuang ShangQing Pills by RP-HPLC[J].Western Journal of Traditional Chinese Medicine,2016,29(10):27.
[7]韦瑀龙,蓝晓庆,黄敏,等.复方感冒颗粒特征图谱与黄芩苷含量测定方法研究[J].西部中医药,2017,30(03):27.
 WEI Yulong,LAN Xiaoqing,HUANG Min,et al.Study on Specific Chromatogram of Compound Cold Granules and the Assay Method of Baicalin Content[J].Western Journal of Traditional Chinese Medicine,2017,30(10):27.
[8]白兆琴,王惠霞,王宏伟△.黄芩苷对胃癌SGC-7901细胞TLR8、HIF-1α、PDGFβ和pten表达的影响[J].西部中医药,2017,30(08):12.
 BAI Zhaoqin,WANG Huixia,WANG Hongwei.The Effects of Baicalin on the Expression of TLR8, HIF-1α, PDGFβ and pten of Gastric Cancer SGC-7901 Cells[J].Western Journal of Traditional Chinese Medicine,2017,30(10):12.
[9]刘光华,于艳,王思源,等.HPLC法同时测定甘露消毒丹中3种成分含量[J].西部中医药,2018,31(09):42.
 LIU Guanghua,YU Yan,WANG Siyuan,et al.The Contents of Three Ingredients in GanLu XiaoDu Pills Determined by HPLC Method Simultaneously[J].Western Journal of Traditional Chinese Medicine,2018,31(10):42.
[10]李会婷,史天陆△,付恩桃,等.RP-HPLC法同时测定咽炎片中黄芩苷和丹皮酚的含量[J].西部中医药,2020,33(01):56.[doi:10.12174/j.issn.1004-6852.2020.01.15]
 LI Huiting,SHI Tianlu,FU Entao,et al.Determination of Baicalin and Paeonol Contained in Pharyngitis Tablets by RP-HPLC Simultaneously[J].Western Journal of Traditional Chinese Medicine,2020,33(10):56.[doi:10.12174/j.issn.1004-6852.2020.01.15]
[11]伍迪,杨雪松,叶建州,等.加味黄连解毒合剂制剂工艺及质量标准研究[J].西部中医药,2020,33(07):38.[doi:10.12174/j.issn.1004-6852.2020.07.09]
 WU Di,YANG Xuesong,YE Jianzhou,et al.Research on Quality Standard and Preparation Technology of Modified Huanglian Jiedu Mixture[J].Western Journal of Traditional Chinese Medicine,2020,33(10):38.[doi:10.12174/j.issn.1004-6852.2020.07.09]

备注/Memo

备注/Memo:
*基金项目:嘉峪关市科技局基金项目(编号2011-38)作者简介:焦正花(1969—),女,副主任药师。研究方向:中药制剂。
更新日期/Last Update: 2014-10-15